State Of Decay Update (2, 3, 4, 5, 6) Crack WORK
State Of Decay Update (2, 3, 4, 5, 6) Crack WORK
State Of Decay Update (2, 3, 4, 5, 6) Crack
as more and more fully understanding of the structure of tm-based cathodes are revealed, it is increasingly possible to control the features and behaviors of specific cathode materials by choosing the appropriate chemical formula. for instance, it has been demonstrated that the filling factor of lithium can be effectively improved by using mos2 as the cathode in order to reduce the formation of dendrites 47, 48 . on the other hand, we also propose a method to inhibit the premature cracks formation, by utilizing the nmc333 cathode materials. nmc333, with a high initial capacity of 119.9 ma h g−1 at 0.1c, was chosen as a representative cathode material. the rate-controlled cell cycling at a high cutoff voltage of 4.7v did not lead to intragranular cracks. only when a cell was cycled at 0.1c, cracks were initiated and grew at a constant rate to eventually penetrate the whole electrode. as the amount of li can be electrochemically extracted from the electrode, it is obvious that the crack growth rate is much faster than the cell voltage change rate. this is the main reason for the constant crack growth rate of the electrodes cycled at 0.1c. it is possible to, therefore, inhibit the formation of intragranular cracks by means of electrochemical cycling at low rate.
in summary, using advanced stem techniques, we report the electrochemical crack initiation mechanism of nmc333 layered cathode materials. we find that the intragranular cracking begins from the interior of the grain, rather than from its grain boundary. through extensive studies, we confirm that the formation of intragranular cracks is an electrochemically driven and diffusion-controlled process. the results in this work provide deep insights into the intragranular cracking process, which may open up a new route to fabricate low cost, high performance lithium-ion batteries.
as more and more fully understanding of the structure of tm-based cathodes are revealed, it is increasingly possible to control the features and behaviors of specific cathode materials by choosing the appropriate chemical formula. for instance, it has been demonstrated that the filling factor of lithium can be effectively improved by using mos2 as the cathode in order to reduce the formation of dendrites 47, 48 . on the other hand, we also propose a method to inhibit the premature cracks formation, by utilizing the nmc333 cathode materials. nmc333, with a high initial capacity of 119.9 ma h g−1 at 0.1c, was chosen as a representative cathode material. the rate-controlled cell cycling at a high cutoff voltage of 4.7v did not lead to intragranular cracks. only when a cell was cycled at 0.1c, cracks were initiated and grew at a constant rate to eventually penetrate the whole electrode. as the amount of li can be electrochemically extracted from the electrode, it is obvious that the crack growth rate is much faster than the cell voltage change rate. this is the main reason for the constant crack growth rate of the electrodes cycled at 0.1c. it is possible to, therefore, inhibit the formation of intragranular cracks by means of electrochemical cycling at low rate.
in summary, using advanced stem techniques, we report the electrochemical crack initiation mechanism of nmc333 layered cathode materials. we find that the intragranular cracking begins from the interior of the grain, rather than from its grain boundary. through extensive studies, we confirm that the formation of intragranular cracks is an electrochemically driven and diffusion-controlled process. the results in this work provide deep insights into the intragranular cracking process, which may open up a new route to fabricate low cost, high performance lithium-ion batteries.
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